Ranjbar, M., Taher, M., Rajaei, P. (2014). Preparation and Characterization of Bismuth Sulfide (Bi2S3) Nanostructures by Ultrasonic Method. Journal of Ultrafine Grained and Nanostructured Materials, 47(1), 15-19. doi: 10.7508/jufgnsm.2014.01.003
Mehdi Ranjbar; Mohammad Ali Taher; Peyman Rajaei. "Preparation and Characterization of Bismuth Sulfide (Bi2S3) Nanostructures by Ultrasonic Method". Journal of Ultrafine Grained and Nanostructured Materials, 47, 1, 2014, 15-19. doi: 10.7508/jufgnsm.2014.01.003
Ranjbar, M., Taher, M., Rajaei, P. (2014). 'Preparation and Characterization of Bismuth Sulfide (Bi2S3) Nanostructures by Ultrasonic Method', Journal of Ultrafine Grained and Nanostructured Materials, 47(1), pp. 15-19. doi: 10.7508/jufgnsm.2014.01.003
Ranjbar, M., Taher, M., Rajaei, P. Preparation and Characterization of Bismuth Sulfide (Bi2S3) Nanostructures by Ultrasonic Method. Journal of Ultrafine Grained and Nanostructured Materials, 2014; 47(1): 15-19. doi: 10.7508/jufgnsm.2014.01.003
Preparation and Characterization of Bismuth Sulfide (Bi2S3) Nanostructures by Ultrasonic Method
1Young Researchers and Elites Club, Kerman Branch, Islamic Azad University, Kerman
2Department of Chemistry, Shahid Bahonar University of Kerman
3Faculty of Science, Kerman Branch, Islamic Azad University, Kerman, Iran.
Abstract
In the present work, Bi2S3 nanostructures have been synthesized with the aid of thioglycollic acid (TGA) a solvent, capping agent, and sulfide source in the presence of ultrasonic method. The as-synthesized products were characterized by X-ray diffraction (XRD), Energy Dispersive X-ray spectroscopy (EDS), scanning electron microscope (SEM), and photoluminescence (PL) spectroscopy. The band gap of nanoparticles calculated 2.37 eV that shows a blue shift compare Bi2S3 bulk. The effects of reaction time and ultrasonic power on the morphology and particle size of product were studied.
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