Strontium carbonate (SrCO3) is one of the most important strontium compounds that have been used in a variety of technological and industrial applications. In the present investigation, nano-structured strontium carbonate was synthesized by mechano-chemical reaction of celestite ore (SrSO4) collected from Dasht-e kavir, Iran and sodium carbonate during high energy mechanical milling.The milling were performed for different durations of time up to 16 hours in a high-energy planetary ball mill with the rotational speed and ball to powder weight ratio of 300 rpm and 30, respectively. X-Ray diffraction (XRD), X-ray fluorescence spectrometer (XRF) and scanning electron microscope (SEM) were used to characterize the obtained samples. XRD results showed that at a Na2CO3:SrSO4 molar ratio of 1.05:1, mechano-chemical reaction started after 1 hour of milling. Although the longer milling times gives a more conversion of SrSO4 to SrCO3 but it has not been completed even after 16 hours of milling. However, by increasing the molar ratio of Na2CO3:SrSO4 to 1.25:1, the SrCO3 formation was completed after 2 hours. The results also showed that the mean crystallites sizes of produced nano-powder were approximately 32 nm. XRF result indicated that the final product was obtained with a purity of 95 wt.%. SEM studies confirmed the formation of SrCO3 nano-powder with a mean particle size of 80 nm.
Alimohammadi, E., Sheibani, S., & Ataie, A. (2018). Preparation of nano-structured strontium carbonate from Dasht-e kavir celestite ore via mechanochemical method. Journal of Ultrafine Grained and Nanostructured Materials, 51(2), 147-152. doi: 10.22059/jufgnsm.2018.02.06
MLA
Erfan Alimohammadi; Saeed Sheibani; Abolghasem Ataie. "Preparation of nano-structured strontium carbonate from Dasht-e kavir celestite ore via mechanochemical method", Journal of Ultrafine Grained and Nanostructured Materials, 51, 2, 2018, 147-152. doi: 10.22059/jufgnsm.2018.02.06
HARVARD
Alimohammadi, E., Sheibani, S., Ataie, A. (2018). 'Preparation of nano-structured strontium carbonate from Dasht-e kavir celestite ore via mechanochemical method', Journal of Ultrafine Grained and Nanostructured Materials, 51(2), pp. 147-152. doi: 10.22059/jufgnsm.2018.02.06
VANCOUVER
Alimohammadi, E., Sheibani, S., Ataie, A. Preparation of nano-structured strontium carbonate from Dasht-e kavir celestite ore via mechanochemical method. Journal of Ultrafine Grained and Nanostructured Materials, 2018; 51(2): 147-152. doi: 10.22059/jufgnsm.2018.02.06